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Faculty of Sciences
Document Details
Document Type
:
Article In Journal
Document Title
:
Synthesis of p-Phenylenediamine from 4-Nitroaniline Using Platinum Doped Lanthanum Hydroxide Nanowires
Synthesis of p-Phenylenediamine from 4-Nitroaniline Using Platinum Doped Lanthanum Hydroxide Nanowires
Document Language
:
English
Abstract
:
A hydrothermal method was used to prepare lanthanum hydroxide nanowires, and a photoassisted deposition method was used to deposit platinum on the surface of the La(OH)(3) nanowires. Various techniques, such as BET, XRD, XPS, PL, UV-Vis, and TEM measurements were employed to characterize the prepared samples. Preparation of p-phenylenediamine by photocatalytic reduction of 4-nitroaniline under visible light irradiation was used to determine the photocatalytic performance of the obtained samples. The results indicate that platinum was well dispersed on the La(OH)(3) nanowire surface. In addition, blocking of some of the pores of the La(OH)(3) nanowires due to deposition of platinum metal leads to the lanthanum hydroxide nanowires with a BET surface area that is higher than that of Pt/La(OH)(3) nanowires. The 0.20 wt% Pt/La(OH)(3) nanowires possessed the lowest band gap and highest photocatalytic activity for the reduction of 4-nitroaniline to p-phenylenediamine under visible light irradiation with stable performance after five reuse
ISSN
:
1533-4880
Journal Name
:
JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY
Volume
:
16
Issue Number
:
9
Publishing Year
:
1437 AH
2016 AD
Article Type
:
Article
Added Date
:
Thursday, August 3, 2017
Researchers
Researcher Name (Arabic)
Researcher Name (English)
Researcher Type
Dr Grade
Email
M (Abdelaal
(Abdelaal, M
Researcher
R Mohamed
Mohamed, R
Researcher
Files
File Name
Type
Description
42434.pdf
pdf
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